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AlCl3催化下C60与脱氢枞胺的胺加成反应

《南京林业大学学报(自然科学版)》[ISSN:1000-2006/CN:32-1161/S]

Issue:
2007年03期
Page:
95-98
Column:
研究论文
publishdate:
2007-03-20

Article Info:/Info

Title:
Amine Addition Reaction of C60with Dehydroabietylamine Catalyzed by AICl3
Article ID:
1000-2006(2007)03-0095-04
Author(s):
GAO Jian1 LIN Zhong-xiang1* DENG Hui-min2
1. College of Chemica! Engineering Nanjing Forestry University, Nanjing 210037, China; 2. Instrumental Apalysis and Research Center, Sun Yat sen University, Guangzhou 510275, China
Keywords:
C60 Dehydroabietylamine Amine addition
Classification number :
TQ351
DOI:
10.3969/j.jssn.1000-2006.2007.03.020
Document Code:
A
Abstract:
In order to obtain Friedel-Crafts adduct of C60 with dehydroabietylamine, the reaction of C60 with dehydroabietylamine was carried out in the presence of AlCl2 in chlorobcn zene at 130 C for 3 d in the dark. The derivatives of C60 were isolated by silica column chromatography and characterized by FT-1R, 13C NMR, 1H NMR, ESI-MS. The results showed that arnine addition reaction between C60 and dehydroabietylamine took place instead of Friedel-Crafts reaction, and a mono-adduct of C60 and dehydroabietylamine obtained as the main product. A new synthesis method of C60 and amino was provided.

References

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Last Update: 2013-05-20