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花生壳苯酚液化的响应面分析及优化工艺(PDF)

《南京林业大学学报(自然科学版)》[ISSN:1000-2006/CN:32-1161/S]

Issue:
2015年06期
Page:
137-142
Column:
研究论文
publishdate:
2015-11-30

Article Info:/Info

Title:
Liquefaction conditions optimization of peanut shell by phenol using response surface analysis
Article ID:
1000-2006(2015)06-0137-06
Author(s):
ZHOU YingLI ZichengSHEN DaZHAO GuominSHEN Weijie ZHOU XiaoyanHAN Shuguang*
College of Materials Science and Engineering, Nanjing Forestry University, Nanjing 210037, China
Keywords:
peanut shell phenol liquefaction response surface methodology
Classification number :
TQ432.9
DOI:
10.3969/j.issn.1000-2006.2015.06.024
Document Code:
A
Abstract:
Response surface analysis was used for the liquefaction conditions optimization of peanut shell liquefaction by phenol and concentrated sulfuric acid. Experimental design and data analysis were performed using by Design-Expert 8.0.6 software. A central composite design was used to investigate the effects of four experimental factors, namely ratio of liquid to solid(mass ratio of phenol and peanut shell), liquefier temperature, liquefier time and catalyst amount on residue ratio, amount of combined formaldehyde and free phenol content of liquefaction products. The results showed that the optimum liquefaction conditions were mass ratio of phenol and peanut shell 3.0, 120 ℃, 80 min and catalyst amount 10 g(per 100 g peanut shells). The residue ratio, amount of combined formaldehyde and free phenol content of liquefaction products under the optimum conditions were 34.11%, 0.65 g and 30.25%, which were almost equal to the predictable value and could provide a reference for peanut shell used in wood industry adhesives.

References

[1] 周建华. 我国花生产业供求、价格与利益分配研究[D]. 北京:中国农业科学院,2012. Zhou J H. China peanut economics:supply and demand, price and distribution of benefits[D]. Beijing:Chinese Academy of Agricultural Sciences,2012.
[2] 周瑞宝. 花生加工技术[M]. 北京: 化学工业出版社,2003.
[3] 孙丰文,张茜,李自峰. 花生壳综合利用的研究进展[J]. 山东林业科技,2008(6):84-88. Sun F W, Zhang Q, Li Z F. Research progress on the comprehensive utilization of peanut hull[J]. Journal of Shandong Forestry Science and Technology,2008(6): 84-88.
[4] 冯辉明, 刘启明, 孙达旺. 花生壳提取物制胶粘剂的研究[J]. 林产化学与工业, 1992, 12(3): 235-239. Feng H M, Liu Q M, Sun D W. Study on adhesive from extracts of peanut hulls[J]. Chemistry and Industry of Forest Products, 1992, 12(3): 235-239.
[5] 常君成, 汪玉秀. 花生壳提取物制造木材用胶粘剂[J]. 中国胶粘剂, 1992,1(3): 13-14. Chang J C,Wang Y X.Preparation of wood adhesive by extracting from peanut hull[J].China Adhesives, 1992,1(3): 13-14.
[6] Chen C M, Winistorfer P M. Effects of molar ratio of formaldehyde to phenol on bonding flakeboards with copolymer resins of peanut hull extracts, phenol, and formaldehyde[J]. Holzforschung, 1993, 47(6): 507-512.
[7] Chen C M, Chen T Y, Dong J. Bonding flakeboard of Taiwanese woods with copolymer resins of peanut hull extracts, phenol and formaldehyde[J]. Holzforschung, 1993, 47(5): 435-438.
[8] Chen C M. Bonding flakeboards of southern species with copolymer resins of forest and agricultural residue extracts[J]. Holzforschung, 1994, 48(6): 517-521.
[9] 李西忠. 花生壳在胶合板生产中的应用[J]. 山东林业科技, 1998(3): 40-42.
[10] Chen C M, Nicholls D L. Room-temperature laminating of CCA-treated lumber with copolymer resins made of biomass extracts[J]. Forest Products Journal, 2000, 50(3): 81-86.
[11] 林巧佳,黄儒珠. 花生壳全粉碱法制胶的初步研究[J]. 福建林学院学报, 1995, 15(3): 208-212. Lin Q J,Huang R Z. Preliminary study on adhesive made from peanut shell with alkaline[J].Journal of Fujian College of Forestry, 1995, 15(3): 208-212.
[12] 刘启明, 薛松, 冯辉明. 花生壳制木材用胶粘剂的研究[J]. 中国胶粘剂, 1994,3(3): 17-21. Liu Q M, Xue S, Feng H M. Research of adhesive for wood from peanut shells[J]. China Adhesives, 1994,3(3): 17-21.
[13] 张茜, 孙丰文, 贺磊, 等. 花生壳苯酚液化物-甲醛树脂胶用于集装箱底板试验[J]. 林业科技开发, 2009, 23(3): 80-83. Zhang Q,Sun F W,He L,et al.Study of peanut shell phenol-liquefaction product formaldehyde resin applied to gluing container floor[J]. China Forestry Science and Technology, 2009, 23(3): 80-83.
[14] 张茜. 花生壳液化及其胶粘剂制备技术[D]. 南京:南京林业大学, 2009. Zhang Q. Liquefaction of peanut hulls and a preparing technique of its resinificaiton[D]. Nanjing:Nanjing Forestry University,2009.
[15] 晏少侠. 苯酚液化花生壳制备胶粘剂及其性能研究[D]. 南京:南京林业大学, 2014. Yan S X. Study on liquefaction of peanut shell in phenol and its properties as wood adhesive[D]. Nanjing:Nanjing Forestry University,2014.
[16] Pan H. Synthesis of polymers from organic solvent liquefied biomass: A review[J]. Renewable & Sustainable Energy Reviews, 2011, 15(7): 3454-3463.
[17] Zhao Y, Yan N, Feng M W. Biobased phenol formaldehyde resins derived from beetle-infested pine barks—Structure and composition[J]. ACS Sustainable Chemistry & Engineering, 2013, 1(1): 91-101.

Last Update: 2015-11-30