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盐析辅助水蒸气蒸馏法制备红松壳挥发油研究(PDF)

《南京林业大学学报(自然科学版)》[ISSN:1000-2006/CN:32-1161/S]

Issue:
2016年06期
Page:
122-128
Column:
研究论文
publishdate:
2016-11-30

Article Info:/Info

Title:
The preparation and component analysis of pine shell volatile oil by salting out-assisted steam distillation
Article ID:
1000-2006(2016)06-0122-07
Author(s):
ZONG FangfangBAO YihongLI Dehai*GUO HongxinXU YingGU Jialin
College of Forestry, Northeast Forestry University, Harbin 150040,China
Keywords:
pine shell salt out-assisted steam distillation volatile oil gas chromatograph/mass spectrom
Classification number :
TQ420
DOI:
10.3969/j.issn.1000-2006.2016.06.019
Document Code:
A
Abstract:
The volatile oil of pine shell was extracted by salt out-assisted steam distillation to discuss effect of inorganic salt in the process of steam distillation. The distillation time, solid-liquid ratio, the inorganic salt type and its concentration, extraction agent on the yield of pine shell volatile oil were studied by single factor tests, while the constituents of pine shell volatile oil was analyzed by the gas chromatograph/mass spectrom(GC/MS). The results showed that the optimized extraction technology of the salting out-assisted steam distillation was distillation time for 3 h, solid-liquid ratio for 1:9(g/mL), best salting out effect was 4×10-3 g/mL disodium hydrogen phosphate. The yield of volatile oil was up to 0.9% under these conditions, that is steam distillation method prepared pine shell volatile oil extraction rate(0.64%)of 1.4 times. The results of pine shell volatile oil components analysis showed that 17 species components in the pine shell volatile oil prepared by salting out-assisted steam distillation were identified by GC/MS, and 16 species components in the pine shell volatile oil prepared by steam distillation. There are the same nine species components in two kinds of essential oil, 2-furanmethanol,5-ethenyltetrahydro-5-trimethyl; benzaldehyde; bicyclo[2.2.1]heptan-2-one, 1,7,7-trimethyl-,(1S); bicyclo[2.2.1]heptan-2-ol,1,7,7-trimethyl; bicyclo[3.1.1]heptan-2-one,6,6-dimethyl-,(1R); bicyclo[3.1.1]heptan-2-one,3,6,6-trimethyl, benzenemethanol,4-trimethyl; bicyclo[3.1.1]hept-3-en-2-one,4,6,6- trimethyl, 2-cyclohexen-1-one,3-methyl-6-(1-methylethenyl). The relative percentage of 9 kinds of components is almost equal.

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Last Update: 2016-11-20