Influence of different extraction methods on the chemical composition of grape pomace condensed tannins

LAN Ping, HUANG Runzhou, ZHOU Dingguo, BROSSE Nicolas, CHRUSCIEL Laurent

JOURNAL OF NANJING FORESTRY UNIVERSITY ›› 2015, Vol. 39 ›› Issue (04) : 105-110.

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JOURNAL OF NANJING FORESTRY UNIVERSITY ›› 2015, Vol. 39 ›› Issue (04) : 105-110. DOI: 10.3969/j.issn.1000-2006.2015.04.018

Influence of different extraction methods on the chemical composition of grape pomace condensed tannins

  • LAN Ping1, HUANG Runzhou1*, ZHOU Dingguo1, BROSSE Nicolas2, CHRUSCIEL Laurent2
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Abstract

Condensed tannins were extracted from grape pomace by acid precipitation and lyophilisation, respectively. Influence of the recovery methods on the chemical structure and composition of tannin extracts was investigated by using Carbon Nuclear Magnetic Resonance(13C-NMR)and Matrix-Assisted Laser Desorption/Ionization Time of Flight(MALDI-TOF)Mass Spectrometry. The results showed that the procyanidin units played a dominait role in two kinds of condensed tannin extracts, and small proportion glucose and gallic acid substitutions bonded in procyanidin units which was linked together by C4-C8 bond. The polymerization degree of acidified condensed tannins was higher than that of lyophilized condensed tannins. In addition, relatively low carbonhydrate and high catechinc acid content in acidified condensed tannins were observed compared with lyophilized condensed tannins. Different extraction methods had great influence on the chemical composition of grape pomace tannin extracts.

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LAN Ping, HUANG Runzhou, ZHOU Dingguo, BROSSE Nicolas, CHRUSCIEL Laurent. Influence of different extraction methods on the chemical composition of grape pomace condensed tannins[J]. JOURNAL OF NANJING FORESTRY UNIVERSITY. 2015, 39(04): 105-110 https://doi.org/10.3969/j.issn.1000-2006.2015.04.018

References

[1] Pizzi A. Condensed tannins for adhesives[J].Ind Eng Chem Prod Res Dev, 1982, 21(3): 359-369.
[2] Vázquez G, Freire S, González J, et al. Characterization of Pinus pinaster bark and its alkaline extracts by diffuse reflectance fourier transform infrared(DRIFT)spectroscopy[J]. Holz als Roh-und Werkstoff, 2000, 58(1): 57-61.
[3] Panamgama L A. Polyphenolic extracts of Pinus radiata bark and networking mechanisms of additive-accelerated polycondensates[J]. Journal of Applied Polymer Science, 2007,103(4):2487-2493.
[4] Fradinho D M, Neto C P, Evtuguin D, et al. Chemical characterization of bark and of alkaline bark extracts from maritime pine grown in Portugal[J]. Industrial Crops and Products, 2002, 16(1): 23-32.
[5] Ping L, Brosse N, Chrusciel L, et al. Extraction of condensed tannins from grape pomace for use as wood adhesives[J]. Industrial Crops and Products, 2011, 33(1): 253-257.
[6] Ping L, Pizzi A, Zhou D G, et al. Condensed tannins extraction from grape pomace: characterization and utilization as wood adhesives for wood particleboard[J]. Industrial Crops and Products, 2011, 34(1): 907-914.
[7] Fu C, Loo A E K, Chia F P P, et al. Oligomeric proanthocyanidins from mangosteen pericarps[J]. Journal of Agriculture and Food Chemistry, 2007, 55(19): 7689-7694.
[8] Hoong Y B, Pizzi A, Tahir P M, et al. Characterization of Acacia mangium polyflavonoid tannins by MALDI-TOF mass spectrometry and CP-MAS 13C NMR[J]. European Polymer Journal, 2010, 46(6): 1268-1277.
[9] Navarrete P, Pizzi A, Pasch H, et al. MALDI-TOF and 13C NMR characterization of maritime pine industrial tannin extract[J]. Industrial Crops and Products, 2010, 32(2): 105-110.
[10] Pizzi A. Advanced wood adhesive technology[M]. New York: Marcel Dekker Inc., 1994, 156-168.
[11] Sears K D, Casebier R L, Hergert H L, et al. The structure of catechinic acid: a base rearrangement product of catechin[J]. J Org Chem, 1974, 39(22): 3244-3247.
[12] Kiatgrajai P, Wellons J D, Gollob L, et al. Kinetics of epimerization of(+)-catechin and its rearrangement to catechinic acid[J]. J Org Chem, 1982, 47(5): 2910-2912.
[13] Monagasa M, López J E Q, Cordovésa C G, et al. MALDI-TOF MS analysis of plant proanthocyanidins[J]. Journal of Pharmaceutical and Biomedical Analysis, 2010, 51(2):358-372.
[14] Reed J D, Krueger C G, Vestling M M. MALDI-TOF mass spectrometry of oligomeric food polyphenols[J]. Phytochemistry, 2005, 66(18): 2248-2263.
[15] Ricardo-Da-Silva J M, Riguad J, Cheynier V, et al. Procyanidin dimers and trimers from grape seeds[J]. Phytochemistry, 1991, 30(4): 1259-1264.
[16] Hoong Y B, Paridah M T, Luqman C A, et al. Fortification of sulfited tannin from the bark of Acacia mangium with phenol-formaldehyde for use as plywood adhesive[J]. Industrial Crops and Products, 2009, 30(3): 416-421.
[17] Pash H, Pizzi A, Rode K. MALDI-TOF mass spectrometry of polyflavonoid tannins[J]. Polymer, 2001, 42(18): 7531-7539.
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